Production instruction | ||||
Production unit: landmarkchem Order object: workshop NO.2 Date: 2014.10.20 | ||||
Voucher No. | 331055897XM | Instruction No. | LMK141020TE | |
Product Name | Testosterone enanthate | Product No. | LM001 | |
Specification | 99% | Quantity | 150kg | |
Launch Date | 2014.10.23 | Expected Completion Date | 2014.10.31 | |
Production Date | 2014.10.23 | Actual finish date | 2014.10.31 | |
Material Usage Note | ||||
Material Name | 4-AD | Recipient date | 2014.10.20 | |
Receive quantity | 1800kg | Actual Quantity | 1652kg | |
Recipient | wang | Quarantine inspector | liu | |
Manufacturing method | ||||
1 Etherification reaction: rate of charge by 4―AD∶ absolute ethyl alcohol∶ triethyl orthoformate∶ Hydrogen pyridine bromide salts = 1∶0.9~1.1∶0.7~0.9∶0.0045~0.0055; generate Etherate via Etherification; 2 Restore hydrolysis reaction: rate of charge by Etherate∶ sodium borohydride or PBH(potassium borohydride)∶ methanol∶ hydrochloric acid∶sodium hydroxide=1∶0.12~0.18∶ 9~11∶0.8~1.2∶ 0.4~0.0.6; generate testosterone via hydrolysis; 3 halogenating reaction: rate of charge by testosterone∶benzene∶ pyridine∶ Heptanoyl chloride∶methanol∶ hydrochloric acid=1∶5.8~6.2∶0.8~1.2∶0.75~0.85∶3.3~3.7∶ 0.5~0.7; generate testosterone enanthate via halogenating. | ||||
Transfer note | ||||
Transfer Unit | landmarkchem | Trabsfer Date | 2014.10.21 | |
Factory director | wang | Production Management Division | liu |
Production instruction | ||||
Production unit: landmarkchem Order object: workshop NO.2 Date: 2014.10.20 | ||||
Voucher No. | 115036679TM | Instruction No. | LMK141020TRAC | |
Product Name | Trenbolone Acetate | Product No. | LM011 | |
Specification | 99% | Quantity | 300kg | |
Launch Date | 2014.10.23 | Expected Completion Date | 2014.10.31 | |
Production Date | 2014.10.23 | Actual finish date | 2014.10.31 | |
Material Usage Note | ||||
Material Name | Estra-4,9-diene-3,17-dione 98% | Recipient date | 2014.10.20 | |
Receive quantity | 400kg | Actual Quantity | 367.2kg | |
Recipient | wang | Quarantine inspector | liu | |
Manufacturing method | ||||
1 Etherification reaction: put methanol into retort, acetylchloride, The female steroid - 4, 9 - diene - 3, 17―diketone, stir, adjust pH value, suction filtration, washing, centrifuge. 2 Restore hydrolysis reaction: add potassium borohydride, stir, adjust pH value, washing, concentration. 3 hydrolysis reaction: add methanol, HCl, base plate,adjust pH value, concentration, add dichloromethane and dissolve, washing, dehydration. 4 dehydrogenation reaction: rinse with dichloromethane, add DDQ, base plate, suction filtration, washing, concentration, cooling, drying, get trenbolone. 5 acylation reaction: suction benzene, pyridine, put into trenbolone, 4-DMAP, dropwise add acetylchloride, heat preservation, washing, concentration, get trenbolone acetate. | ||||
Transfer note | ||||
Transfer Unit | landmarkchem | Trabsfer Date | 2014.10.21 | |
Factory director | wang | Production Management Division | liu |